Efficacy of FTIR Analysis in Determining CO2 Loading on Diglycolamine

dc.creatorHuang, Roger
dc.creatorSilveria, Mark
dc.creatorKong, Jessica
dc.creatorBelancik, Grace
dc.creatorJan, Darrell
dc.date.accessioned2018-07-08T00:29:47Z
dc.date.available2018-07-08T00:29:47Z
dc.date.issued2018-07-08
dc.descriptionRoger Huang, NASA
dc.descriptionMark Silveria, Independent
dc.descriptionJessica Kong, NASA
dc.descriptionGrace Belancik, NASA
dc.descriptionDarrell Jan, NASA
dc.descriptionICES302: Physio-chemical Life Support- Air Revitalization Systems -Technology and Process Development
dc.descriptionThe 48th International Conference on Environmental Systems was held in Albuquerque, New Mexico, USA on 08 July 2018 through 12 July 2018.
dc.description.abstractIn support of advanced air revitalization technologies to enable human spaceflight beyond low earth orbit, performance studies have been conducted using a liquid amine, Diglycolamine (DGA) between teams at NASA’s Johnson Spaceflight Center (JSC) and Ames Research Center (ARC). Liquid amines have been used in regenerable earth-based systems to remove CO2 from industrial systems as well as for closed-environment air revitalization because they can be regenerated at lower temperatures than solid sorbent systems. As an additional advantage to solid sorbent-based systems, liquid sorbents can be cycled between an adsorbing contactor and degassing chamber, thereby reducing system complexity by operation in a continuous loop. In an effort to inform a regeneration system design for micro-gravity applications, ARC has performed a number of tests to characterize the degas mechanics of DGA. In order to accurately measure the amount of CO2 captured or released by the amine, methods such as gravimetric weighing and chemical desorption are reasonable, however the first iteration test setup for a scaled down degas system required analysis on small sample sizes. Fourier-transform infrared spectroscopy (FTIR) analysis was experimentally evaluated to analyze CO2 concentration because it can produce measurements with sample sizes on the order of 100’s of μL. Calibration against chemical desorption showed relatively good correlation and test data showed reasonable adherence to expected trends, however more extensive testing should be conducted to fully validate the usage of FTIR to determine CO2 loading on DGA.en_US
dc.identifier.otherICES_2018_262
dc.identifier.urihttp://hdl.handle.net/2346/74210
dc.language.isoengen_US
dc.publisher48th International Conference on Environmental Systemsen_US
dc.subjectFourier transform infrared spectroscopy
dc.subjectAir revitalization
dc.subjectLiquid amine sorbent
dc.titleEfficacy of FTIR Analysis in Determining CO2 Loading on Diglycolamineen_US
dc.typePresentationen_US

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